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Special Report


       of 80.6% with an average of 94.7% for  tions were done. (Ind. Eng. Chem. Res.,  Highly-efficient acetylene (A)
       each step. (ACS Sus. Chem. Eng., 2024;  2024; DOI: 10.1021/acs.iecr.4c00895).  synthesis by selective electro-
       DOI: 10.1021/acssuschemeng.4c01826).                               chemical formation of CO -
                                         Shaping futures: a dialogue on   derived CaC                   2
                                                                                       2
       Experimental methods in   Chemical Engineering (CE)                [German chemical industry grew in
       Chemical  Engineering:  Education (CEE)                            earlier years, through Reppe Chemistry,
       Karl-Fischer (KF) titration                                        which needs A for a variety of chemicals
                                         P. Chintalapati, G. Evans, D. Gladwin;  that included acetaldehyde, ethylene,
       The moisture determination is con-  M. Jamieson, and N. Ellis have covered  vinyl chloride/acetate, vinyl acetylene
       ducted by KF method extensively. P.  the title subject outlining the importance  and butadiene. A came from CaC  by the
                                                                                                    2
       Rivera-Quintero et al have covered this  of Engineering as a discipline, profes-  standard electrothermal kiln process).
       subject. These authors have given de-  sion, practice, and area of study, to solve
       tails and have pointed out that the main  complex problems faced by humanity.  Y. Suzuki et al have come out with an
                                                           CE does indeed  interesting and a novel way where an
                                                           remain one of  electrothermal formation of calcium
                                                           the vital dis-  carbide (CC) (CaC ) is carried out by
                                                                                          2
                                                           ciplines in the  CO  in NaCl-KCl-CaCl -CaO melt. The
                                                           contemporary      2               2
                                                           world and is not
                                                           only central to
                                                           technological
                                                           advances in key
                                                           areas such as
                                                           energy, medicine,
                                                           and sustainability,
                                                           but also to get
                                                           adaptive changes.
                                                           The curricula
                                                           are witnessing
                                                           enormous chal-
                                                           lenges to remain
                                                           relevant particu-
       sources of error affecting the analysis   larly for future demands. Curricula from
       are ambient moisture, pH, solvent, sample   several institutions have been analysed.
       handling, and titration speed. (Can.  Transferable skills are very important.
       J. Chem. Eng., 2024; DOI: 10.1002/
       cjce.25295).                      This treatise is extensive, and anyone
                                         interested in CE and chemical allied in-
       A green oxidation process for  dustries should read this paper. A historical
       p-xylene (PX) to terephthalic  perspective is also given. Theoretical
       acid (TA) through the UV ir-  framework and methodology are given.
       radiation – enhanced ozonation
       process                           There is a discussion on how CEE can
                                         adopt to an increasingly complex world.
       F. Yuan et al have come out with the  Further, in what way CEE equip students
       title process for the multi-million tonnes  to face the future challenges. The impact
       per annum of TA, where the traditional  of Artificial Intelligence through design is  current efficiency of this method is 92%.
       process involves harsh conditions. Here,  covered and systems approaches can be  The higher crystallinity of carbon led to
       acetonitrile is used as a solvent and  adopted. CEE must adopt to changing  more selective formation of CC. (Chem.
       ozone and UV irradiation are exploited.  complex system. (Can. J. Chem. Eng.,  Eng. Jl., 2024, 494, 15 August, 153013;
       Optimisation was done and DFT calcula-  2024; DOI: 10.1002/cje.25205).  DOI: 10.1016/j.cej.2024.153013).


       172                                                                Chemical Weekly  September 10, 2024


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