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Special Report                                                                   Special Report



 ChemProTech India 2024 – Exhibitor Showcase  of Chemicals Market and New Appli-  sion cladded on carbon steel. The clad
       cations, NobelClad.
                                         tensile  strength  exceeds  the  substrate
 hemProTech India, the leading   Institute  of  Chemical Technology  fl uids  and  slurries.  The  company  has   shear strength by 100%. Also, the weld
 exhibition for the process tech-  (ICT), Mumbai.  fi led a Indian Patent application for this   NobelClad  offers  explosion  weld-  has high corrosion resistance.
 Cnology and equipment industry,   pump.  ing  and  cladding  services  across  all
 and its co-located shows – ChemExpo   A fl ow reactor is completely diffe-  industry sectors. The company has ma-  The  company  has  also  introduced
 India and ChemLogistics India – were   rent than a conventional batch reactor.   A novel microreactor has been de-  jor locations in the USA and Germany,  another  innovation  called  Tantalum
 attended by nearly 25,000 visitors with   There  are  two  major  strategies  used  signed  for  strongly  exothermic  reac-  and offi ces all over the world. Some of  clad.  Tantalum  is  ideal  for  most  se-
 530 exhibitors over the two days, Apirl   in chemicals manufacturing – product  tions.  It  has  a  volume  of  450-ml  and   the markets or industry sectors served  vere  corrosive  situations  and  is  the
 24-25. The show also included several   strategy  and  process  strategy.  Gene-  offers excellent heat transfer and mass   by the company are – chemicals, petro-  metal  of  choice  in  installations  where
 platforms wherein exhibitors could en-  rally,  the  process  strategy  is  used  for  transfer  performance.  Indian  patent   chemicals,  oil & gas, mining, metals,  the glass-lined equipment is subject to
 gage in educative sessions with inter-  chemical  products  with  established  application has been fi led for this novel   marine,  defense,  refrigeration,  power  mechanical shock and thermal failures.
 ested visitors. The Exhibitor Showcases   market. There  is  a  need  to  use  multi-  microreactor, as well.  generation  including  nuclear  power,  Metallography  of  macro-  and  micro-
 ran through  both  days  and  were  well   disciplinary team of chemists, chemical   and  transportation.  The  company  also  specimens of direct tantalum clad plates
 attended.  engineers,  mechanical  engineers,  etc.   Novel  agitated  fl ow  reactors  have   offers  clad  solutions  for  innovative  with  just  1mm  clad  thickness  were   Mr. Bhavesh Shah
 at the design stage of fl ow reactors.   been  designed  for  viscous  fl uids  and   technologies  like  geothermal  energy,  shown. It is possible to fabricate large
 In the following pages, Dr. Ajit Joshi   dense slurries. These are tubular reac-  plastics  recycling,  lithium,  hydrogen  equipment with tantalum cladding.  and  offers  high  effi ciency,  optimized
 (drjoshi9@gmail.com), who conducted   For  designing  a  fl ow  reactor  for  tors  without  any  partitions,  but  they   and carbon capture.  fl ow.  The  process  output  undergoes
 the proceedings, presents an overview   converting a batch process to a conti-  behave like ten stirred tank reactors in   DetaPipeis  a  corrosion-resistant  purifi cation to obtain pure nitrobenzene.
 of the second session held on April 25.   nuous  one,  the  fi rst  step  is  the  study  series.  This  agitated  fl ow  reactor  has   DetaClad is a proprietary explosion  clad pipe spool system. It is a fabricated  The benzene stripping process recovers
 [Reports  on  the  fi rst  session  was   of  chemical  kinetics  of  the  chemical  narrower  residence  time  distribution,   welding process for welding two diffe-  carbon steel pipe. Straight pipes, Ts and  about  60-70%  of  benzene.  There  are
 published in  Chemical Weekly Dated   reactions  involved.  The  second  stage  and much greater heat transfer coeffi -  rent  metals  together.  It  is  purely  an  elbows  can  also  be  made  with  these  several safety features of this process.
 June 18, and the third session will   involves design and simulation, based  cient, leading to better thermal regula-  engineering  exercise.  The  two  metal  pipes. In the coming years, large-scale  Counter-measures are in place to avoid
 follow in a forthcoming edition.  on  the  fl ow  properties,  hydrodynamics,  tion. Indian patent application has been   plates to be joined together are placed  commercialization  of  the  DetaPipe  runaway reactions. It has process-inte-
 etc.  The  use  of  straight  tubes  and  fi led  for  this  agitated  fl ow  reactor  as   at  a  certain  distance  from  each  other  products is expected.   grated temperature control.
 Innovations in fl ow   pinched tubes offer different results for  well.  and  explosive  is  placed  between  the   Mr. Ahlavadi also discussed various   The  KBR  adiabatic  process  offers
       plates.  The  explosive  is  detonated
 mass transfer during the reactions. The
 technology  third  step  involves  techno-economic   DetaClad&DetaPipe –   across the plates. The collision between  Nobelclad solutions for nitric acid and  several advantages over the isothermal
 Dr.  Vishwanath  Dalvi,  Consultant,   analysis, while the fourth step is pilot-  the metal plates generates a jet at the  ammonium nitrate applications.  process,  including  10-15%  lower  cost
 Amar  Equipment  Pvt.  Ltd.,  Assistant   ing or carrying out the process at pilot   Clad solutions for   interface  joining  them.  The  DetaClad   of production.
 Professor  in  Chemical  Engineering,   scale. This is used just to validate the   nitric acid and nitrate   process  creates  lasting  bonds  the  fi rst   Improving energy effi ci-
 fl ow reactor design. It is interesting to   time, no matter what the size or metal   Various  materials  of  construction
 note that some or all of the reactor sec-  applications  combination of the plates.   ency in the production  are  used  to  make  reactors  for  diffe-
 tions used in the pilot plant can later be   Mukesh Ahlavadi, Global Director   of  nitrobenzene  and   rent  KBR  technologies  –  tantalum,
 incorporated  in  the  commercial  scale   Mr. Ahlavadi also presented several   titanium,  silicon  carbide,  glass-lining,
 plant. The  last  or  the  fi fth  step  is  the   cladding  innovations  –  470  LI  –  Su- nitrochlorobenzene by  PTFE-lining,  etc.  for  these  types  of
 establishment  of  a  commercial  scale   perferritic  stainless  steel  alloy,  which   adiabatic nitration tech-  reactions.  Stainless  steel  is  used  rarely
 fl ow reactor plant.  has about 22.25% chromium (Cr) and                  in this application.
       less than 1% nickel (Ni). The chemical   nology
 The market demand of the product   composition of 470 LI, various useful   Bhavesh Shah, Director – Techno- Technology  commer-
 being manufactured decides the length   properties,  such  as  intra-granular  cor-  logy,  KBR  Inorganics  Technology   cialization challenges
 of campaign or manufacturing time in   rosion  resistance,  shear  test  results  as   Solutions, KBR Group.
 the  fl ow  reactor.  The  process  can  be   per  ASTM  A264,  as  well  as  various   and ways to overcome
 operated  in  a  continuous  mode. Also,   research  papers  published  about  this   In  the  KBR  adiabatic  process  for
 multiple  products  can  be  produced   alloy,  and  its  comparison  with  stain-  nitration of benzene, a tubular reactor is  them”.
 in  the  same  fl ow  reactor  in  separate,   less  steels  SS304  and  SS316L,  were  used to carry out the exothermic reac-  Dr.  D.  Shailaja,  Chief  Scientist  &
 continuous campaigns.   discussed  in  detail.  Metallography  of  tion. The heat produced in the process  Chair,  Business  Development  &  Re-
       macro and micro specimens of the weld  is used to re-concentrate the dilute sul-  search Management, Indian Institute of
 Recently, a multipurpose pump has   showed continuous waves, but no micro-  phuric acid generated as a by-product  Chemical Technology (IICT), Hyderabad.
 been  developed  at  Amar  Equipment,   cracks,  even  with  100X  magnifi ca-  during the reaction. The adiabatic pro-
 Dr. Vishwanath Dalvi  which can be used for diffi cult-to-pump   Mr. Mukesh Ahlavadi  tion. 470 LI can be successfully explo-  cess  minimizes  by-product  formation,   In  today’s  VUCA  (Volatile,  Un-

 178  Chemical Weekly  June 25, 2024  Chemical Weekly  June 25, 2024                                   179


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