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Special Report                                                                                                                                                                   Special Report



       ChemProTech India 2024 – Exhibitor Showcase                                                                   of Chemicals Market and New Appli-  sion cladded on carbon steel. The clad
                                                                                                                     cations, NobelClad.
                                                                                                                                                       tensile  strength  exceeds  the  substrate
             hemProTech India, the leading   Institute  of  Chemical Technology  fl uids  and  slurries.  The  company  has                             shear strength by 100%. Also, the weld
             exhibition for the process tech-  (ICT), Mumbai.             fi led a Indian Patent application for this    NobelClad  offers  explosion  weld-  has high corrosion resistance.
       Cnology and equipment industry,                                    pump.                                      ing  and  cladding  services  across  all
       and its co-located shows – ChemExpo   A fl ow reactor is completely diffe-                                     industry sectors. The company has ma-  The  company  has  also  introduced
       India and ChemLogistics India – were   rent than a conventional batch reactor.   A novel microreactor has been de-  jor locations in the USA and Germany,  another  innovation  called  Tantalum
       attended by nearly 25,000 visitors with   There  are  two  major  strategies  used  signed  for  strongly  exothermic  reac-  and offi ces all over the world. Some of  clad.  Tantalum  is  ideal  for  most  se-
       530 exhibitors over the two days, Apirl   in chemicals manufacturing – product  tions.  It  has  a  volume  of  450-ml  and   the markets or industry sectors served  vere  corrosive  situations  and  is  the
       24-25. The show also included several   strategy  and  process  strategy.  Gene-  offers excellent heat transfer and mass   by the company are – chemicals, petro-  metal  of  choice  in  installations  where
       platforms wherein exhibitors could en-  rally,  the  process  strategy  is  used  for  transfer  performance.  Indian  patent   chemicals,  oil & gas, mining, metals,  the glass-lined equipment is subject to
       gage in educative sessions with inter-  chemical  products  with  established  application has been fi led for this novel   marine,  defense,  refrigeration,  power  mechanical shock and thermal failures.
       ested visitors. The Exhibitor Showcases   market. There  is  a  need  to  use  multi-  microreactor, as well.  generation  including  nuclear  power,  Metallography  of  macro-  and  micro-
       ran through  both  days  and  were  well   disciplinary team of chemists, chemical                            and  transportation.  The  company  also  specimens of direct tantalum clad plates
       attended.                         engineers,  mechanical  engineers,  etc.   Novel  agitated  fl ow  reactors  have   offers  clad  solutions  for  innovative  with  just  1mm  clad  thickness  were   Mr. Bhavesh Shah
                                         at the design stage of fl ow reactors.   been  designed  for  viscous  fl uids  and   technologies  like  geothermal  energy,  shown. It is possible to fabricate large
          In the following pages, Dr. Ajit Joshi                          dense slurries. These are tubular reac-    plastics  recycling,  lithium,  hydrogen  equipment with tantalum cladding.  and  offers  high  effi ciency,  optimized
       (drjoshi9@gmail.com), who conducted   For  designing  a  fl ow  reactor  for  tors  without  any  partitions,  but  they   and carbon capture.                                     fl ow.  The  process  output  undergoes
       the proceedings, presents an overview   converting a batch process to a conti-  behave like ten stirred tank reactors in                           DetaPipeis  a  corrosion-resistant  purifi cation to obtain pure nitrobenzene.
       of the second session held on April 25.   nuous  one,  the  fi rst  step  is  the  study  series.  This  agitated  fl ow  reactor  has   DetaClad is a proprietary explosion  clad pipe spool system. It is a fabricated  The benzene stripping process recovers
       [Reports  on  the  fi rst  session  was   of  chemical  kinetics  of  the  chemical  narrower  residence  time  distribution,   welding process for welding two diffe-  carbon steel pipe. Straight pipes, Ts and  about  60-70%  of  benzene.  There  are
       published in  Chemical Weekly Dated   reactions  involved.  The  second  stage  and much greater heat transfer coeffi -  rent  metals  together.  It  is  purely  an  elbows  can  also  be  made  with  these  several safety features of this process.
       June 18, and the third session will   involves design and simulation, based  cient, leading to better thermal regula-  engineering  exercise.  The  two  metal  pipes. In the coming years, large-scale  Counter-measures are in place to avoid
       follow in a forthcoming edition.  on  the  fl ow  properties,  hydrodynamics,  tion. Indian patent application has been   plates to be joined together are placed  commercialization  of  the  DetaPipe  runaway reactions. It has process-inte-
                                         etc.  The  use  of  straight  tubes  and  fi led  for  this  agitated  fl ow  reactor  as   at  a  certain  distance  from  each  other  products is expected.   grated temperature control.
       Innovations in fl ow               pinched tubes offer different results for  well.                            and  explosive  is  placed  between  the   Mr. Ahlavadi also discussed various   The  KBR  adiabatic  process  offers
                                                                                                                     plates.  The  explosive  is  detonated
                                         mass transfer during the reactions. The
       technology                        third  step  involves  techno-economic   DetaClad&DetaPipe –                across the plates. The collision between  Nobelclad solutions for nitric acid and  several advantages over the isothermal
          Dr.  Vishwanath  Dalvi,  Consultant,   analysis, while the fourth step is pilot-                           the metal plates generates a jet at the  ammonium nitrate applications.  process,  including  10-15%  lower  cost
       Amar  Equipment  Pvt.  Ltd.,  Assistant   ing or carrying out the process at pilot   Clad solutions for       interface  joining  them.  The  DetaClad                            of production.
       Professor  in  Chemical  Engineering,   scale. This is used just to validate the   nitric acid and nitrate    process  creates  lasting  bonds  the  fi rst   Improving energy effi ci-
                                         fl ow reactor design. It is interesting to                                   time, no matter what the size or metal                                 Various  materials  of  construction
                                         note that some or all of the reactor sec-  applications                     combination of the plates.        ency in the production  are  used  to  make  reactors  for  diffe-
                                         tions used in the pilot plant can later be   Mukesh Ahlavadi, Global Director                                 of  nitrobenzene  and             rent  KBR  technologies  –  tantalum,
                                         incorporated  in  the  commercial  scale                                       Mr. Ahlavadi also presented several                              titanium,  silicon  carbide,  glass-lining,
                                         plant. The  last  or  the  fi fth  step  is  the                             cladding  innovations  –  470  LI  –  Su- nitrochlorobenzene by  PTFE-lining,  etc.  for  these  types  of
                                         establishment  of  a  commercial  scale                                     perferritic  stainless  steel  alloy,  which   adiabatic nitration tech-  reactions.  Stainless  steel  is  used  rarely
                                         fl ow reactor plant.                                                         has about 22.25% chromium (Cr) and                                  in this application.
                                                                                                                     less than 1% nickel (Ni). The chemical   nology
                                           The market demand of the product                                          composition of 470 LI, various useful   Bhavesh Shah, Director – Techno- Technology  commer-
                                         being manufactured decides the length                                       properties,  such  as  intra-granular  cor-  logy,  KBR  Inorganics  Technology   cialization challenges
                                         of campaign or manufacturing time in                                        rosion  resistance,  shear  test  results  as   Solutions, KBR Group.
                                         the  fl ow  reactor.  The  process  can  be                                  per  ASTM  A264,  as  well  as  various                             and ways to overcome
                                         operated  in  a  continuous  mode. Also,                                    research  papers  published  about  this   In  the  KBR  adiabatic  process  for
                                         multiple  products  can  be  produced                                       alloy,  and  its  comparison  with  stain-  nitration of benzene, a tubular reactor is  them”.
                                         in  the  same  fl ow  reactor  in  separate,                                 less  steels  SS304  and  SS316L,  were  used to carry out the exothermic reac-  Dr.  D.  Shailaja,  Chief  Scientist  &
                                         continuous campaigns.                                                       discussed  in  detail.  Metallography  of  tion. The heat produced in the process  Chair,  Business  Development  &  Re-
                                                                                                                     macro and micro specimens of the weld  is used to re-concentrate the dilute sul-  search Management, Indian Institute of
                                           Recently, a multipurpose pump has                                         showed continuous waves, but no micro-  phuric acid generated as a by-product  Chemical Technology (IICT), Hyderabad.
                                         been  developed  at  Amar  Equipment,                                       cracks,  even  with  100X  magnifi ca-  during the reaction. The adiabatic pro-
               Dr. Vishwanath Dalvi      which can be used for diffi cult-to-pump   Mr. Mukesh Ahlavadi               tion. 470 LI can be successfully explo-  cess  minimizes  by-product  formation,   In  today’s  VUCA  (Volatile,  Un-

       178                                                                     Chemical Weekly  June 25, 2024        Chemical Weekly  June 25, 2024                                                                  179


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